薄荷醇在“南海Ⅰ号”饱水木质文物上安全脱除方法的实验室研究
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(1.北京科技大学科技史与文化遗产研究院,北京 100083;2.国家文物局考古研究中心,北京 100013)

作者简介:

黄琦钧(1997—),女,北京科技大学科技史与文化遗产研究院硕士研究生,研究方向为水下文物提取和保护,E-mail: 1005841184@qq.com 通信作者:韩向娜,副教授,E-mail: jayna422@ustb.edu.cn

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国家重点研发计划资助(2020YFC1521804;2020YFC1521803;2020YFC1522404),中央高校基本科研业务费资助(FRF-MP-20-53)


Laboratory study of technologies for menthol removal from waterlogged archaeological wood of the Nanhai Ⅰ shipwreck
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(1. Institute of Cultural Heritage and History of Science & Technology, University of Science and Technology Beijing, Beijing 100083, China;2. National Centre for Archaeology, Beijing 100013, China)

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    摘要:

    薄荷醇作为新兴的考古出土脆弱文物提取用临时固型材料,在越来越多的考古现场得到了应用,涉及文物材质不断增多,但是文物提取到室内之后薄荷醇如何快速、安全脱除成为后期处理时面临的实际难题。最常用的去除方法是让薄荷醇自然挥发,但是薄荷醇挥发的同时,水分也会挥发;随着水分的挥发,对失水敏感的饱水有机质文物将会出现干缩等问题。为研究薄荷醇在饱水木质文物上的安全脱除技术,本研究以“南海Ⅰ号”沉船出水的饱水树皮和糟朽散木为对象,探讨自然挥发、补水挥发、乙醇去除、乙醇去除+补水、加热+补水5种不同的脱除方法,通过评估不同方法处理前后树皮和散木的外观形态、质量损失和尺寸稳定性,优选出适合饱水木质文物上薄荷醇的安全脱除方法。结果显示:树皮脱除薄荷醇需要补水,散木脱除薄荷醇需要乙醇快速去除。 综合效果来看,乙醇去除或者乙醇去除+补水相结合的方式是饱水木质文物最佳的薄荷醇安全去除方法。本研究将为考古和文物保护人员在使用薄荷醇提取饱水木质文物后期处理上提供技术参考。

    Abstract:

    As a novel temporary consolidant for extracting fragile relics from archaeological sites, menthol has been increasingly applied to many different relics at many excavation sites; however, after relics have been lifted and transported to labs, how to remove previously-used menthol quickly and safely becomes a new challenge. The most commonly-used removal method is to let menthol volatilize naturally, but water also volatilizes when menthol volatilizes. With the loss of water, waterlogged organic relics, which are sensitive to water loss, will have a shrinkage problem. In order to find safe technologies for menthol removal from waterlogged archaeological wood, two types of waterlogged wood relics from the Nanhai Ⅰ shipwreck—bark and rotten wood, which are extremely sensitive to water loss, were taken as examples in our work to test 5 different methods for menthol removal. These methods included natural volatilization, water supplementation+natural volatilization, removal by ethanol, removal by ethanol+water supplementation and water supplementation+heating. The appearance, mass loss and dimensional stability of the tested wood samples were evaluated to select safe methods for menthol removal from waterlogged archaeological wood. The results show that the method of water supplementation worked best for the bark and that of removal by ethanol worked best for the rotten wood. According to the removal effects, ethanol or a combination of ethanol and water are the best methods for the safe removal of menthol from waterlogged wooden relics. This study could provide technological guidance or a reference for archaeologists and conservators in terms of how to remove menthol after its uses for waterlogged archaeological wood.

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  • 收稿日期:2021-04-15
  • 最后修改日期:2021-09-29
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  • 在线发布日期: 2022-08-08
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